有机化学实验（英文版）

Part 1 Basic Knowledge in Organic Chemistry Laboratory

1．1 Rules in laboratory

1．2 Prevention and treatment of the common accidents in laboratory

1．3 Requirements of preparation， record and report of experiments

1．4 Common lab equipment and apparatus

1．5 Waste disposal

Part 2 Basic Experimental Techniques

2．1 Preparation of organic compounds

2．2 The determination of physical constants of organic compounds

2．3 Separation and purification technology of organic compounds

2．4 Spectral analysis technology of organic compounds

Part 3 Experiments for Preparation of Organic Compound

3．1 Preparation of cyclohexene

3．2 Preparation of anhydrous ethanol

3．3 Preparation of n-butyl bromide

3．4 Preparation of n-butyl ether

3．5 Preparation of acetophenone

3．6 Preparation of aspirin

3．7 Preparation of cinnanfic acid

3．8 Preparation of n-butyl acetate

3．9 Preparation of isoamyl acetate

3．10 Synthesis of glycerol monostearate

3．11 Preparation of skin care cosmetic

3．12 Preparation of detergent

Part 4 Extraction， Separation and Identification of

Organic Compounds

4．1 Distilling 95% ethanol and measuring the boiling point

4．2 Recrystallization of benzoic acid

4．3 Purification of benzaldehyde

4．4 Isolation of caffeine from tea leaves

4．5 The extraction of limonene from orange peels

4．6 Separation of A and B by thin-layer chromatography

4．7 Separation of spinach pigments by column chromatography

4．8 Preparation and resolution for optical isomers of tris（ethylenediamine）

cobalt salts

4．9 Identification of sugar

4．10 Identification of amino acids and proteins

Reference

Appendix： Experimental Graphs and Properties of

Organic Solvents

I ． Distilling 95% ethanol and measuring the boiling point

II． Recrystallization of benzoic acid

III． Isolation of caffeine from tea leaves and sublimation

IV． Synthesis， isolation and purification of n-butyl acetate

V． Physical constant